The Madarasz Book. The Secret of the Skill of Madarasz by Louis Madarasz

By Louis Madarasz

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Pieces of a brittle agglomerate may break off, indicating a first failure. However, it is possible that most of the agglomerate remains intact and, after some densification between (3a) and (4), can be compressed further until final catastrophic disintegration occurs at (5). Plastic agglomerates, on the other hand, may never come apart. After considerable densification (between (3) and (6)) the compression force may increase more or less steeply, indicating formation of a less compressible cake.

However, this is not always necessary. Different maximum moisture levels exist that depend on the material. It was found during microscopic studies that caking usually resulted from bonding by the crystals of soluble salts. These crystals often covered the entire granule surface in the form of a veneer or hull. Those salts migrated to the surface of the granule as a solution, leaving numerous small cavities within. Since this mechanism requires water, drying should reduce caking. Some materials respond favorably to several days of curing prior to bagging.

For that reason, very dilute suspensions are used. Nevertheless, it is possible that agglomerates form or conglomerates that are already present do not disintegrate completely. Therefore, dispersion aids are often added, which reduce particle affinity. The molecules of dispersion aids attach to the particles, eliminating polarities and/or reducing interfacial tensions. Separation forces, such as ultrasonic vibrations, can be also introduced for improved disagglomeration and dispersion. In connection with particle size analysis, the importance of correct sample preparation must be stressed.

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